Materials Characterization-I

Course Code:

MSN 220

Course Period:

Spring

Course Type:

Core

Credits:

3

Theoric:

2

Practice:

0

Laboratory Hour:

2

ECTS:

6

Course Language:

English

Course Objectives:

This course serves as an introduction to material characterization. Information will be given regarding material characterization tools such as spectroscopy and mathematical tools will be presented leading towards understanding and analyzing materials in great detail.

Course Content:

Introduction to electron microscopy, beam sources, dedectors, X Ray Diffraction (XRD), X Ray Photoelectron Spectroscopy (XPS), Atomic Force Microscopy (AFM). Optical microscopy

Course Methodology:

1: Lecture by instructor, 2: Lecture by instructor with class discussion, 3: Problem solving by instructor, 4: Use of simulations, 5: Problem solving assignment, 6: Reading assignment, 7: Laboratory work, 8: Term research paper, 9: Presentation by guest

Course Evaluation Methods:

A: Written exam, B: Multiple-choice exam C: Take-home quiz, D: Experiment report, E: Homework, F: Project, G: Presentation by student, H: …

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Course Learning Outcomes

Course Learning Outcomes	Detailed Program Outcomes	Teaching Methods	Assessment Methods
Ability to define the components and functions of characterization tools (XRD, SEM, AFM,…)	1a	1	A, E
Ability to use X-ray diffraction technique to determine the crystal structure of the material	1a, 1b	1, 3, 5	A, E
To be able to explain characterization techniques developed with the help of material knowledge and basic sciences	1b, 2b	1, 6	A, E
Ability to select proper tools to solve common problems for materials characterizations	2b, 4b	1, 6	A, E
Ability to relate and interpret the obtained characterization data with the basic principles of the technique used	1b, 5b	1, 3, 6	A, E

Course Flow

COURSE CONTENT
Week	Topics	Study Materials
1	XRD Powder characterization (Crystal Lattice Structure, Miller Indices)	Textbook and lecture notes
2	XRD Powder characterization (Braggs Law, Peak Analysis and Indexing)	Textbook and lecture notes
3	XRD Powder characterization (Particle Size Analysis with Scherrer Equation)	Textbook and lecture notes
4	Fundamentals of Electron Microscopy (SEM, TEM, EDX, Interaction of electron with sample)	Textbook and lecture notes
5	Configuration of Electron Microscopy	Textbook and lecture notes
6	Configuration of Electron Microscopy	Textbook and lecture notes
7	Sample Preparation for Analysis (Lab)	Textbook and lecture notes
8	Atomic Force Microscopy, Scanning Tunneling Microscopy	Textbook and lecture notes
9	Midterm
10	SAED Electron Diffraction	Textbook and lecture notes
11	SAED Electron Diffraction	Textbook and lecture notes
12	Thermal Characterization DTA-TGA	Textbook and lecture notes
13	Thermal Characterization (Type of thermocouples - case study - homework)	Textbook and lecture notes
14	Sample Preparation for Analysis (Lab)	Textbook and lecture notes
15	Final

Material Sharing

MATERIAL SHARING
Documents	Textbook and lecture notes
Assignments	Homeworks
Exams	Exams and solutions

Assessment

ASSESSMENT
IN-TERM STUDIES	NUMBER	PERCENTAGE
Midterm	1	30
Homework	4	30

Total		60
CONTRIBUTION OF FINAL EXAMINATION TO OVERALL GRADE		40
CONTRIBUTION OF IN-TERM STUDIES TO OVERALL GRADE		60
Total		100

Course’s Contribution to Program

COURSE'S CONTRIBUTION TO PROGRAM OUTCOMES
No	Program Learning Outcomes	check √
1a	Adequate knowledge in mathematics, science and engineering subjects pertaining to the relevant discipline,	√
1b	Ability to use theoretical and applied knowledge in these areas in complex engineering problems.	√
2a	Ability to identify, formulate, and solve complex engineering problems,
2b	Ability to select and apply proper analysis and modeling methods for this purpose.	√
3a	Ability to design a complex system, process, device or product under realistic constraints and conditions, in such a way as to meet the desired result,
3b	Ability to apply modern design methods for this purpose.
4a	Ability to devise, select and use modern techniques and tools needed for analyzing and solving complex problems encountered in engineering practice.
4b	Ability to employ information technologies effectively.	√
5a	Ability to design experiments for investigating complex engineering problems or discipline specific research questions,
5b	Ability to conduct experiments, gather data, analyze and interpret results for investigating complex engineering problems or discipline specific research questions.	√
6a	Ability to work efficiently in intra-disciplinary teams,
6b	Ability to work efficiently in multi-disciplinary teams,
6c	Ability to work individually.
7a	Ability to communicate effectively in Turkish, both orally and in writing,
7b	Knowledge of a minimum of one foreign language,
7c	Ability to write effective reports and comprehend written reports, prepare design and production reports,
7d	Ability to make effective presentations,
7e	Ability to give and receive clear and intelligible instructions.
8a	Recognition of the need for lifelong learning, ability to access information, ability to follow developments in science and technology,
8b	Ability to continue to educate him/herself.
9a	Consciousness to behave according to ethical principles and professional and ethical responsibility.
9b	Knowledge on standards used in engineering practice.
10a	Knowledge about business life practices such as project management, risk management, change management.
10b	Awareness in entrepreneurship and innovation.
10c	Knowledge about sustainable development.
11a	Knowledge about the global and social effects of engineering practices on health, environment, and safety,
11b	Knowledge about contemporary issues of the century reflected into the field of engineering.
11c	Awareness of the legal consequences of engineering solutions.

ECTS

ECTS ALLOCATED BASED ON STUDENT WORKLOAD BY THE COURSE DESCRIPTION
Activities	Quantity	Duration (Hour)	Total Workload (Hour)
Course Duration	14	4	56
Hours for off-the-classroom study (Pre-study, practice)	14	6	84
Midterm Examinations	1	3	3
Final Examinations	1	3	3

Total Work Load			146
Total Work Load / 25 (h)			5,84
ECTS Credit of the Course			6

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Materials Characterization-I

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