Analytical Chemistry

Course Code:

CHEM215

Course Period:

Spring

Course Type:

Core

Credits:

4

Theoric:

3

Practice:

0

Laboratory Hour:

2

ECTS:

6

Course Language:

English

Course Objectives:

1. To provide the students with the ability to analyze and interpret the results and/or data of experiments/analyses/research using traditional methods (such as classical genetics calculations) as well as computer technologies (such as bioinformatics methods) 2. To ensure that the to-be engineers are able to communicate in contemporary topics in GBE, who are successful particularly in oral and written communication, who can carry our teamwork and interdisciplinary studies, responsible, innovative, entrepreneurs that are self-confident and can compete in their fields, who comply with ethics and environmental issues. 3. To seed the concepts of lifelong education, learning and self-improvement, to ensure that they be individuals with self-improvement capabilities 4. To ensure the perception of the impact of bioengineering and biotechnology at the global and social levels, and to raise individuals who can provide novel and innovative solutions (so as to increase our international competitiveness) to these problems

Course Content:

1)Fundamentals of Analytical Chemistry 2)Using Spreadsheets and Calculations Used in Analytical Chemistry 3) Errors in Chemical Analyses 4)Statistical Evaluation of Analytical Data 5)Gravimetric and Titrimetric Methods of Analysis 6)Aqueous Solutions Chemistry 7)Activities and Activity Coefficients 8)Potentiometric Methods 9)Introduction to Spectrochemical Methods 10)Instruments for Optical Spectrometry 11) Molecular Absorption Spectroscopy 12)Molecular Fluorescence Spectroscopy 13) Nuclear Magnetic Resonance 14)Mass Spectroscopy 15)Kinetic Methods of Analysis 16)Introduction to Analytical Separations 17)High-Performance Liquid Chromatography 18)Electrophoresis and modes of electrophoresis 19)Gas Chromatography

Course Methodology:

1: Lecture by instructor, 2: Lecture by instructor with class discussion, 3: Problem solving by instructor, 4: Use of simulations, 5: Problem solving assignment, 6: Reading assignment, 7: Laboratory work, 8: Term research paper, 9: Presentation by guest s

Course Evaluation Methods:

A: Written exam, B: Multiple-choice exam C: Take-home quiz, D: Experiment report, E: Homework, F: Project, G: Presentation by student, H: …

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Course Learning Outcomes

Course Learning Outcomes	Detailed Program Outcomes	Teaching Methods	Assessment Methods
Explain the fundamentals of analytical chemistry and steps of a characteristic analysis.	Expresses the role of analytical chemistry in science. Compare qualitative and quantitative analyses. Expresses the quantitative analysis methods. Expresses the qualitative analysis methods.	1, 7	A, D
2. Evaluate the analytical data in terms of statistics.	Estimates kinds of errors in chemical analysis. Evaluates the effects of systematic errors on analytical results. Compare of the experimental mean with a true value and two experimental means. Determine the detection limits. Interpret the statistical tests.	1, 3, 5, 7	A, D
3. Interpret the sources of random error and its effect on analytical results.	Explain the sources of random errors. Specifies the standard deviation of calculated results. Expresses the significant figures and rounding of data. Define the general properties of volumetry Employ the volumetric calculations.	1, 3, 5, 7	A, D
4. Identify quality of experimental measurements.	Explain the confidence level and confidence limit. Identifies the detection limit. Interprets statistical tests. Describe the salts and the buffer solutions	1, 2, 3, 5, 7	A, D
5. Interpret aqueous solution chemistry.	Expresses the terms such as electrolyte, acid, base, conjugate acid/base and auto pyrolysis. Explains the chemical equilibrium and equilibrium constant types. Describes the activity coefficient and properties of activity coefficient.	1, 3, 5, 7	A, D
6. Apply the equilibrium calculations to complex systems.	Determines systematic method for solving the multiple-equilibrium problems. Identifies the solubility by the systematic method. Solves the problems related to ion separation by control of the concentration of the precipitating reagents.	1, 3, 5, 7	A, D
7. Learn the separation and purification of an organic mixture by chemical/solvent separation methods.	Students will understand the fundamentals of principles of chromatographic techniques. Students will develop basic skills in the techniques of crystallization, distillation, solvent extraction, and thin layer, column, liquid, gas chromatography and in quantitative dilution. Enable the students in biomolecule preparations.	1, 2, 3, 5, 7	A, D
8. Get a deep insight into the various spectroscopic methods used for the characterization of bio macromolecules.	To know the basics principle of different techniques employed in molecular spectroscopy · To study the fundamentals, instrumentation and important applications of UV, Fluorescence, and Mass and NMR Spectroscopy.	1, 3, 5, 7	A, D

Course Flow

COURSE CONTENT
Week	Topics	Study Materials
1	Fundamentals of Analytical Chemistry	Textbook
2	Using Spreadsheets in Analytical Chemistry Calculations Used in Analytical Chemistry	Calculator, Computer
3	Errors in Chemical Analyses Statistical Evaluation of Analytical Data	Textbook, Calculator
4	Sampling, Standardization, Calibration and Validation	Textbook, Calculator
5	Potentiometry pH Measurement	Textbook, Calculator
6	Chemical Equilibria Aqueous Solutions and Chemical Equilibria Effect of Electrolytes on Chemical Equilibria	Textbook, Calculator
7	Spectrochemical Methods Introduction to Spectrochemical Methods Instruments for Optical Spectrometry	Textbook
8	Molecular Absorption Spectrometry Molecular Fluorescence Spectroscopy	Textbook
9	Nuclear Magnetic Resonance (NMR)	Textbook
10	Mass Spectroscopy	Textbook
11	Kinetics and Separations Introduction to Analytical Separations	Textbook
12	High-Performance Liquid Chromatography Electrophoresis and modes of electrophoresis Gas Chromatography	Textbook

Recommended Sources

RECOMMENDED SOURCES
Textbook	Fundamentals of Analytical Chemistry, Skoog, West, Holler, and Crouch, 8th Edition (International Student Edition)
Additional Resources	Quantitative Chemical Analysis, Daniel C. Harris, 8th edition, W. H. Freeman and Company, 2010

Material Sharing

MATERIAL SHARING
Documents	Brief notes related to course
Assignments	Laboratory Conduct, Laboratory Report, Attendance
Exams	Midterm, Final, Pop quiz, Pre Lab quiz

Assessment

ASSESSMENT
IN-TERM STUDIES	NUMBER	PERCENTAGE
Midterm exam	2	30%
Pop Quizzes	2	15%
Laboratory Laboratory Conduct (15 points) • Pre-Lab Quiz (15 points) • Check out (30 points) • Laboratory Report (40 points)	11	20%
Total	15	35%
CONTRIBUTION OF FINAL EXAMINATION TO OVERALL GRADE	1	35%
CONTRIBUTION OF IN-TERM STUDIES TO OVERALL GRADE	15	65%
Total	16	100

Course’s Contribution to Program

COURSE'S CONTRIBUTION TO PROGRAM OUTCOMES
No	Program Learning Outcomes	check √
1a	Adequate knowledge in mathematics, science and engineering subjects pertaining to the relevant discipline,	√
1b	Ability to use theoretical and applied knowledge in these areas in complex engineering problems.	√
2a	Ability to identify, formulate, and solve complex engineering problems,	√
2b	Ability to select and apply proper analysis and modeling methods for this purpose.
3a	Ability to design a complex system, process, device or product under realistic constraints and conditions, in such a way as to meet the desired result,	√
3b	Ability to apply modern design methods for this purpose.
4a	Ability to devise, select and use modern techniques and tools needed for analyzing and solving complex problems encountered in engineering practice.	√
4b	Ability to employ information technologies effectively.
5a	Ability to design experiments for investigating complex engineering problems or discipline specific research questions,	√
5b	Ability to conduct experiments, gather data, analyze and interpret results for investigating complex engineering problems or discipline specific research questions.
6a	Ability to work efficiently in intra-disciplinary teams,	√
6b	Ability to work efficiently in multi-disciplinary teams,	√
6c	Ability to work individually.	√
7a	Ability to communicate effectively in Turkish, both orally and in writing,
7b	Knowledge of a minimum of one foreign language,
7c	Ability to write effective reports and comprehend written reports, prepare design and production reports,	√
7d	Ability to make effective presentations,
7e	Ability to give and receive clear and intelligible instructions.
8a	Recognition of the need for lifelong learning, ability to access information, ability to follow developments in science and technology,	√
8b	Ability to continue to educate him/herself.	√
9a	Consciousness to behave according to ethical principles and professional and ethical responsibility.
9b	Knowledge on standards used in engineering practice.	√
10a	Knowledge about business life practices such as project management, risk management, change management.
10b	Awareness in entrepreneurship and innovation.
10c	Knowledge about sustainable development.
11a	Knowledge about the global and social effects of engineering practices on health, environment, and safety,
11b	Knowledge about contemporary issues of the century reflected into the field of engineering.
11c	Awareness of the legal consequences of engineering solutions.

ECTS

ECTS ALLOCATED BASED ON STUDENT WORKLOAD BY THE COURSE DESCRIPTION
Activities	Quantity	Duration (Hour)	Total Workload (Hour)
Course Duration	6	3	3
Hours for off-the-classroom study (Pre-study, practice)	4	2	2
Total Work Load	10	5	5
Total Work Load / 25 (h)
ECTS Credit of the Course	6.0

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Analytical Chemistry

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