Instrumental Methods Of Analysis

Course Code:

CHBE415

Course Type:

Area Elective

Credits:

3

Theoric:

3

Practice:

0

Laboratory Hour:

0

ECTS:

5

Course Language:

English

Courses given by:

Semin Funda Oğuz

Course Objectives:

The aim of this course is teaching modern instrumentation techniques and meanwhile supplying the theoretical knowledge beyond these techniques, the application boundaries and rules, important points to be taken into account and expertise of the interpretation of the data. Contribution of the Course to the Professional Education: Gaining Competency to Follow and Organize the Chemical Analyses Processes

Course Content:

Application and theory of modern instrumentation techniques, principles of instrumental analysis, atomic spectroscopy, molecular spectroscopy, chromatographic separation and various methods, possibilities and limitations in different methods and instrumental techniques, applications, observations, applicability, qualitative and quantitative measurements of chemical properties.

Course Methodology:

1: Lecture by instructor, 2: Lecture by instructor with class discussion, 3: Problem solving by instructor, 4: Use of simulations, 5: Problem solving assignment, 6: Reading assignment, 7: Laboratory work, 8: Term research paper, 9: Presentation by guest

Course Evaluation Methods:

A: Written exam, B: Multiple-choice examC:Take-home quiz, D: Experiment report, E: Homework, F: Project, G: Presentation by student

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Course Learning Outcomes

Course Learning Outcomes	Detailed Program Outcomes	Teaching Methods	Assessment Methods
1) Ability to understand the working principles of modern instrumentations	1 a	1,2, 3	A,B
2) Ability to define application areas of instrumentation techniques	4 a	1, 2	A, B
3) Ability to observe and apply the instrumentation techniques	5 b,6 a, c	7	A, D
4) Ability to interpret the instrumental analyses results	5 b, 7 b, c	1, 7	A, D
5) Ability to follow the improvements in instrumentation techniques	7 d, 8 a, b	1, 8	F, G

Course Flow

COURSE CONTENT
Week	Topics	Study Materials
1	Introduction to Molecular Spectroscopy	Textbook
2	UV/VIS Spectroscopy	Textbook
3	IR Spectroscopy	Textbook
4	IR Spectroscopy	Textbook
5	NMR Spectroscopy	Textbook
6	NMR Spectroscopy	Textbook
7	Mass Spectrometry	Textbook
8	Atomic Absorption Spectrometry	Textbook
9	Scanning Electron Microscopy	Textbook
10	Separation Techniques and High Pressure Liquid Chromatography	Textbook
11	High Pressure Liquid Chromatography	Textbook
12	Gas Chromatography	Textbook
13	Differential Thermal Analysis and Differential Scanning Calorimetry	Textbook
14	Presentations	Textbook

Recommended Sources

RECOMMENDED SOURCES
Textbook	Skoog, Holler and Niemann, ”Principles of Instrumental Analysis”, 5th Edition, Brooks/Cole
Additional Resources	Rouessac F. and Rouessac A., “Chemical Analysis, Modern Instrumentation Methods and Techniques”, 2nd Edition, Wiley

Material Sharing

https://yulearn.yeditepe.edu.tr/course presentation slides

Assessment

ASSESSMENT
IN-TERM STUDIES	NUMBER	PERCENTAGE
Mid-term	1	58
Lab quizes/homework	5	17
Lab Report	5	25
Term Project Presentation (extra points)	1	(8)
Total		100
CONTRIBUTION OF FINAL EXAMINATION TO OVERALL GRADE		40
CONTRIBUTION OF IN-TERM STUDIES TO OVERALL GRADE		60
Total		100

Course’s Contribution to Program

COURSE'S CONTRIBUTION TO PROGRAM OUTCOMES
No	Program Learning Outcomes	check √
1a	Adequate knowledge in mathematics, science and engineering subjects pertaining to the relevant discipline,	√
1b	Ability to use theoretical and applied knowledge in these areas in complex engineering problems.
2a	Ability to identify, formulate, and solve complex engineering problems,
2b	Ability to select and apply proper analysis and modeling methods for this purpose.
3a	Ability to design a complex system, process, device or product under realistic constraints and conditions, in such a way as to meet the desired result,
3b	Ability to apply modern design methods for this purpose.
4a	Ability to devise, select and use modern techniques and tools needed for analyzing and solving complex problems encountered in engineering practice.	√
4b	Ability to employ information technologies effectively.
5a	Ability to design experiments for investigating complex engineering problems or discipline specific research questions,
5b	Ability to conduct experiments, gather data, analyze and interpret results for investigating complex engineering problems or discipline specific research questions.	√
6a	Ability to work efficiently in intra-disciplinary teams,	√
6b	Ability to work efficiently in multi-disciplinary teams,
6c	Ability to work individually.	√
7a	Ability to communicate effectively in Turkish, both orally and in writing,
7b	Knowledge of a minimum of one foreign language,	√
7c	Ability to write effective reports and comprehend written reports, prepare design and production reports,	√
7d	Ability to make effective presentations,	√
7e	Ability to give and receive clear and intelligible instructions.
8a	Recognition of the need for lifelong learning, ability to access information, ability to follow developments in science and technology,	√
8b	Ability to continue to educate him/herself.
9a	Consciousness to behave according to ethical principles and professional and ethical responsibility.
9b	Knowledge on standards used in engineering practice.
10a	Knowledge about business life practices such as project management, risk management, change management.
10b	Awareness in entrepreneurship and innovation.
10c	Knowledge about sustainable development.
11a	Knowledge about the global and social effects of engineering practices on health, environment, and safety,
11b	Knowledge about contemporary issues of the century reflected into the field of engineering.
11c	Awareness of the legal consequences of engineering solutions.

ECTS

ECTS ALLOCATED BASED ON STUDENT WORKLOAD BY THE COURSE DESCRIPTION
Activities	Quantity	Duration (Hour)	Total Workload (Hour)
Course Duration	14	3	42
Hours for off-the-classroom study (Pre-study, practice)	14	2	28
Midterm examination	1	2	2
Laboratory quizes	5	3	15
Laboratory Reports / Homework	5	5	25
Project	1	15	15
Final examination	1	2	2
Total Work Load			129
Total Work Load / 25 (h)			5.2
ECTS Credit of the Course			5

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Instrumental Methods Of Analysis

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